Test of pasting

[SubhaRDas]

SPECTROSCOPY
ExperimentNMR
Example applications include: 1D NMR spectra for various nuclei (1H, 13C, 19F, 31P) and Water suppression techniques (WATERGATE, Excitation sculpting, Presaturation)
ExperimentNMR2D
Example applications include: Correlation Spectroscopy (COSY), Double Quantum Filtered COSY (DQF-COSY), COSY-β, Total Correlation Spectroscopy (TOCSY), Heteronuclear Multiple Bond Correlation (HMBC), Heteronuclear Single Quantum Coherence (HSQC), HSQC-TOCSY, Heteronuclear Multiple Quantum Coherence (HMQC), HMQC-TOCSY, Nuclear Overhauser Effect Spectroscopy (NOESY), Rotational Frame Nuclear Overhauser Effect Spectroscopy (ROESY)
500 MHz NMR
11.74 T Magnet
500 MHz for ¹H
126 MHz for ¹³C
202 MHz for ³¹P
470 MHz for ¹⁹F
Probe
SmartProbe ¹H/¹⁹F/¹³C/³¹P 5 mm probe (-150°C to 150°C)
Inverse Triple Resonance (TXI) ¹H/¹³C/¹⁹N 5 mm probe (-150°C to 150°C)
Autosampler
6 to 51°C incubation temperature
480 NMR tubes per batch
Standard NMR tubes hold 600 µL to 1.5 mL
Micro NMR tubes hold 40 µL
2D Experiment Types
Correlation spectroscopy (COSY)
Double-quantum filtered COSY
COSY featuring a 45 degree pulse
Total correlation spectroscopy (TOCSY)
Heteronuclear single quantum correlation spectroscopy (HSQC, 1H-13C or 1H-15N)
Heteronuclear multiple quantum correlation spectroscopy (HMQC)
Heteronuclear multiple-bond correlation spectroscopy (HMBC, 1H-13C or 1H-15N)
HSQC-TOCSY (1H-13C)
HMQC-TOCSY (1H-13C)
Nuclear Overhauser effect spectroscopy (NOESY)
Rotating-frame Overhauser effect spectroscopy (ROESY)
Bruker Ascend 500